(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

Base Information

Chemical Name:(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine
CAS No.:1071509-14-2
Molecular Formula:C₃₉H₄₅NO₄Si
Molecular Weight:619.876
Hs Code.:

Synonyms:(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

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Chemical Property of (2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

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Technology Process of (2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

There total 1 articles about (2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1071509-07-3
(2R,4S,6S)-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

: 98-88-4
benzoyl chloride

: 1071509-14-2
(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1002/ejoc.200800348

Reference yield: 65.0%

: 1071509-14-2
(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine

: 1071509-16-4
(2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-6-phenylpiperidine-2-carboxylic acid

Guidance literature:: (2R,4S,6S)-N-benzoyl-4-tert-butyldiphenylsiloxy-2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-6-phenylpiperidine; With periodic acid; In diethyl ether; at 20 ℃; for 4h;

With sodium chlorite; sodium dihydrogenphosphate; In water; acetonitrile; at 0 ℃; for 0.0833333h;

With dihydrogen peroxide; In water; acetonitrile; at 0 ℃; for 1h;
DOI:10.1002/ejoc.200800348