1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan

Base Information

• Chemical Name: 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan
• CAS No.: 162967-97-7
• Molecular Formula: C₄₈H₄₀N₂P₄
• Molecular Weight: 768.754

Synonyms:1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan

Chemical Property of 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan

Chemical Property:

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Technology Process of 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan

There total 5 articles about 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?³λ³)diphospha-3,4-(?⁴λ⁵)diphosphahexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

Lithium-bis(diphenylphosphanyl)amid (73785-70-3) → 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?3λ3)diphospha-3,4-(?4λ5)diphosphahexan (162967-97-7)

Guidance literature:

With iodine; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1039/c39950000037

Reference yield: 52.0%

Bis(diphenylphosphanyl)amine (2960-37-4) → 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?3λ3)diphospha-3,4-(?4λ5)diphosphahexan (162967-97-7)

Guidance literature:

With iron(III) trifluoride; n-butyllithium; In tetrahydrofuran; hexane; 1.) 15 min, 2.) r.t., 45 min;

DOI:10.1515/znb-1996-0206

Reference yield:

Lithium-bis(diphenylphosphanyl)methanid (28926-61-6) + Lithium-bis(diphenylphosphanyl)amid (73785-70-3) → C50H42P4 (153647-81-5) + C50H42P4 + C49H41NP4 + 1,1,3,3,4,4,6,6-Octaphenyl-2,5-diaza-1,6-(?3λ3)diphospha-3,4-(?4λ5)diphosphahexan (162967-97-7)

Guidance literature:

With iodine; In tetrahydrofuran; at -40 ℃;

DOI:10.1039/c39950000037

upstream raw materials:

Lithium-bis(diphenylphosphanyl)methanid

Lithium-bis(diphenylphosphanyl)amid

Bis(diphenylphosphanyl)amine

Downstream raw materials:

(C₆H₅)2P(Se)NP(C₆H₅)2P(C₆H₅)2NP(Se)(C₆H₅)2

imidotetraphenyldiphosphinic acid

[(AuCl)2((C₆H₅)2PNP(C₆H₅)2P(C₆H₅)2NP(C₆H₅)2)]

[PtCl₂((C₆H₅)2PNP(C₆H₅)2P(C₆H₅)2NP(C₆H₅)2)]

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