2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

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Chemical Name:2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2
CAS No.:1184174-93-3
Molecular Formula:C₁₆H₁₇ClN₄O
Molecular Weight:318.774
Hs Code.:

Synonyms:2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

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Chemical Property of 2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

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Technology Process of 2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

There total 3 articles about 2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: chloroacetic acid-d3

: 4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-1,2,3,6-tetrahydropyridine dihydrochloride

: 1184174-93-3
2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

Guidance literature:: chloroacetic acid-d3; With oxalyl dichloride; N,N-dimethyl-formamide; In toluene; at 0 - 20 ℃; for 1h;

4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-1,2,3,6-tetrahydropyridine dihydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; at 0 - 20 ℃; for 1h;

Reference yield: 20.0%

: 1633-48-3
chloroacetic acid-d₂

: 4-[4-(1-methyl-1H-[1,2,4]triazol-3-yl)-pheny|]-1,2,3,6-tetrahydropyridine hydrochloride

: 1184174-93-3
2-Chloro-1-(4-(4-(1-methyl-1H-1,2,4-triazol-3-yl)phenyl)-3,6-dihydropyridin-1(2H)-yl)ethan-1-one-2,2-d2

Guidance literature:: 2-chloro-2,2-dideuterio-acetic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In toluene; at 0 - 20 ℃; for 1h;

4-[4-(1-methyl-1H-[1,2,4]triazol-3-yl)-pheny|]-1,2,3,6-tetrahydropyridine hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; at 0 - 20 ℃; for 1h;