N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

Base Information

Chemical Name:N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide
CAS No.:927663-59-0
Molecular Formula:C₂₉H₃₁N₃O₆
Molecular Weight:517.582
Hs Code.:

Synonyms:N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

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Technology Process of N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

There total 3 articles about N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 105-36-2
ethyl bromoacetate

: 612836-81-4
N-ethyl-4-(4-aminobenzylamino)-1,8-naphthalimide

: 927663-59-0
N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1039/b309569j

Reference yield:

: 4403-71-8
(4-aminomethyl)aniline

: 927663-59-0
N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0.17 h / 130 °C

1.2: 90 percent / 0.5 h

2.1: 90 percent / KI; K₂CO₃ / dimethylformamide / 90 °C

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1039/b309569j

Reference yield:

: 100874-09-7
6-bromo-2-ethyl-1H-benzo[de]isoquinoline-1,3(2H)dione

: 927663-59-0
N-ethyl-4-{4-[bis(ethoxycarbonylmethyl)amino]benzylamino}-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0.17 h / 130 °C

1.2: 90 percent / 0.5 h

2.1: 90 percent / KI; K₂CO₃ / dimethylformamide / 90 °C

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1039/b309569j