2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone

Base Information

• Chemical Name: 2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone
• CAS No.: 809274-89-3
• Molecular Formula: C₁₅H₂₆O₄Si₂
• Molecular Weight: 326.54

Synonyms:2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone

Chemical Property of 2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone

Chemical Property:

Purity/Quality:

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Technology Process of 2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone

There total 1 articles about 2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2,3-dimethoxy-4-(3-trimethylsilyl-1-propynyl)-4-trimethylsilyloxycyclobut-2-en-1-one → 2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone (809274-89-3)

Guidance literature:

In para-xylene; at 138 ℃; for 1h;

DOI:10.1016/j.tet.2004.09.052

Reference yield: 30.0%

2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone (809274-89-3) + ethanol (64-17-5) → 2,3-dimethoxy-6-ethoxymethyl-5-trimethylsilyl-1,4-benzoquinone + 2,3-dimethoxy-5-(ethoxymethyl)-1,4-benzoquinone (127998-61-2)

Guidance literature:

2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone; ethanol; for 2h; Heating;

With silver(l) oxide; In benzene; at 20 ℃; for 0.25h;

DOI:10.1016/j.tet.2004.09.052

Reference yield:

2,3-dimethoxy-5-trimethylsilyl-6-((trimethylsilyl)methyl)-1,4-benzoquinone (809274-89-3) → 2-bromo-5,6-dimethoxy-3-trimethylsilanylmethyl-benzene-1,4-diol

Guidance literature:

With hydrogen bromide; In dichloromethane; for 0.0833333h;

DOI:10.1016/j.tet.2004.09.052

Downstream raw materials:

2,3-dimethoxy-5-(ethoxymethyl)-1,4-benzoquinone

5-bromo-2,3-dimethoxy-6-((trimethylsilyl)methyl)-1,4-benzoquinone

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