Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

Base Information

Chemical Name:Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside
CAS No.:136179-31-2
Molecular Formula:C₄₀H₄₂O₁₆
Molecular Weight:778.764
Hs Code.:

Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O-<methyl (2,3,4-tri-O-acetyl-β-D-glucopyranosyl)uronate>-β-D-galactopyranoside

Synonyms:Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

Suppliers and Price of Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

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Technology Process of Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

There total 1 articles about Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117181-25-6
Benzyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 136179-31-2
Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; iodine; silver carbonate; Yield given. Multistep reaction; 1) CH₂Cl₂, 1 h, r.t. 2) CH₂Cl₂, 3 d;
DOI:10.1016/0008-6215(91)84027-C

Reference yield: 92.0%

: 136179-31-2
Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

: 136179-32-3
Benzyl 2-O-benzoyl-3-O--β-D-galactopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/0008-6215(91)84027-C

Reference yield:

: 136179-31-2
Benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O--β-D-galactopyranoside

: 136597-46-1
Benzyl 3-O-(β-D-glucopyranosyl uronate)-4,6-di-O-sulfo-β-D-galactopyranoside, trisodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / aq. 90percent CF₃CO₂H / CH₂Cl₂ / 0.5 h / 0 °C

2: 1) Me₃N*SO₃ 2) Et₃N / 1) DMF, 2 d, r.t. 2) toluene

3: 94 percent / 1M aq. NaOH / tetrahydrofuran / 0 °C

With sodium hydroxide; sulfur trioxide trimethylamine complex; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0008-6215(91)84027-C