C₂₃H₁₇IO₃

Base Information

Chemical Name:C₂₃H₁₇IO₃
CAS No.:1587718-86-2
Molecular Formula:C₂₃H₁₇IO₃
Molecular Weight:468.291
Hs Code.:

C<sub>23</sub>H<sub>17</sub>IO<sub>3</sub>

Synonyms:C₂₃H₁₇IO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₇IO₃

Chemical Property:

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Technology Process of C₂₃H₁₇IO₃

There total 4 articles about C₂₃H₁₇IO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1587718-67-9
1-(3',4-dimethoxy[1,1'-biphenyl]-2-yl)-3-phenylprop-2-yn-1-one

: 1587718-86-2
C₂₃H₁₇IO₃

Guidance literature:: With disodium hydrogenphosphate; Iodine monochloride; In acetonitrile; at 20 ℃; for 1h; regioselective reaction;
DOI:10.1021/jo5001803

Reference yield:

: 56658-04-9
2-bromo-5-methoxybenzoyl chloride

: 1587718-86-2
C₂₃H₁₇IO₃

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

3: disodium hydrogenphosphate; Iodine monochloride / acetonitrile / 1 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; disodium hydrogenphosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Iodine monochloride; caesium carbonate; triethylamine; In tetrahydrofuran; acetonitrile; 1: |Sonogashira Cross-Coupling / 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo5001803

Reference yield:

: 134419-78-6
1-(2-bromo-5-methoxyphenyl)-3-phenylprop-2-yn-1-one

: 1587718-86-2
C₂₃H₁₇IO₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

2: disodium hydrogenphosphate; Iodine monochloride / acetonitrile / 1 h / 20 °C

With disodium hydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Iodine monochloride; caesium carbonate; In tetrahydrofuran; acetonitrile; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo5001803