1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene

Base Information

• Chemical Name: 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropa
• Molecular Formula: C₁₇H₁₄Cl₂S
• Molecular Weight: 321.27

Synonyms:1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene

Chemical Property of 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropa

Chemical Property:

Purity/Quality:

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Useful:

There total 3 articles about 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Ethyl trichloroacetate (515-84-4) + (3,4-dihydronaphthalen-1-yl)(phenyl)sulfane (68243-21-0) → 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene (126745-21-9)

Guidance literature:

DOI:10.1002/hlca.19890720723

Reference yield: 82.0%

(3,4-dihydronaphthalen-1-yl)(phenyl)sulfane (68243-21-0) + sodium trichloroacetate (650-51-1) → 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene (126745-21-9)

Guidance literature:

DOI:10.1002/hlca.19890720723

Reference yield: 53.0%

(3,4-dihydronaphthalen-1-yl)(phenyl)sulfane (68243-21-0) + phenyltrichloromethylmercury (3294-57-3) → 1,1-dichloro-1a,2,3,7b-tetrahydro-7b-(phenylthio)-1H-cyclopropanaphthalene (126745-21-9)

Guidance literature:

In benzene; for 14h; Ambient temperature;

DOI:10.1002/hlca.19890720723

upstream raw materials:

Ethyl trichloroacetate

(3,4-dihydronaphthalen-1-yl)(phenyl)sulfane

sodium trichloroacetate

phenyltrichloromethylmercury

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