tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

Base Information

Chemical Name:tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate
CAS No.:1226869-16-4
Molecular Formula:C₁₈H₂₂O₃
Molecular Weight:286.371
Hs Code.:

Synonyms:tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

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Chemical Property of tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

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Technology Process of tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

There total 1 articles about tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1227303-99-2
2-methylene-6-phenylhex-5-yn-1-ol

: 80994-44-1
{[(tert-butoxycarbonyl)oxy]amino}(phenyl)acetonitrile

: 1226869-16-4
tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

Guidance literature:: 2-methylene-6-phenylhex-5-yn-1-ol; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h;

{[(tert-butoxycarbonyl)oxy]amino}(phenyl)acetonitrile; In tetrahydrofuran; diethyl ether; hexane; at 0 - 20 ℃;
DOI:10.5012/bkcs.2010.31.03.670

Reference yield: 91.0%

: 1226869-16-4
tert-butyl 2-methylene-6-phenylhex-5-ynyl carbonate

: 1227303-78-7
C₁₄H₁₄O₃

Guidance literature:: With silver hexafluoroantimonate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; In 1,2-dichloro-ethane; at 20 ℃; for 0.333333h; diastereoselective reaction;
DOI:10.5012/bkcs.2010.31.03.670