2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate

Base Information

• Chemical Name: 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate
• CAS No.: 24760-81-4
• Molecular Formula: C₁₅H₁₅NO₆S
• Molecular Weight: 337.353
• Mol file: 24760-81-4.mol

Synonyms:2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate

Chemical Property of 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate

There total 2 articles about 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-Methoxyphenyl)ethanol (702-23-8) + 4-Nitrobenzenesulfonyl chloride (98-74-8) → 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate (24760-81-4)

Guidance literature:

Multistep reaction; (i) MeLi, hexane, Et₂O, (ii) /BRN= 746543/;

DOI:10.1021/jo00946a010

Reference yield:

→ 2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate (24760-81-4)

Guidance literature:

2-p-Anisylethanol, p-Nitrobenzolsulfonylchlorid;

DOI:10.1039/J29710000498

Reference yield:

2-(p-methoxyphenyl)ethyl p-nitrobenzenesulphonate (24760-81-4) + p-toluidine (106-49-0,12221-03-3) → p-nitrobenzenesulfonic acid (138-42-1) + N-[2-(4-methoxyphenyl)ethyl]-4-methylaniline

Guidance literature:

In methanol; at 65 ℃; Mechanism; Rate constant;

DOI:10.1039/P29880001537

upstream raw materials:

2-(4-Methoxyphenyl)ethanol

4-Nitrobenzenesulfonyl chloride

Downstream raw materials:

p-nitrobenzenesulfonic acid

N-(2-(4-Methoxyphenyl)ethyl)aniline