1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

Base Information

Chemical Name:1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester
CAS No.:97188-46-0
Molecular Formula:C₁₆H₁₅F₅NO₃
Molecular Weight:364.292
Hs Code.:

Synonyms:1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

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Chemical Property of 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

Chemical Property:

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Technology Process of 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

There total 1 articles about 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 38632-29-0
1-Oxyl-1,2,5,6-tetrahydro-2,2,6,6-tetramethylpyridin-4-carboxylic acid radical

: 97188-46-0
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 3h; Ambient temperature;

Reference yield:

: 97188-46-0
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

: 97188-52-8
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaBH₄ / ethanol / 1 h / 0 °C

2: 76 percent / pyridine / 3 h / 5 °C

With pyridine; sodium tetrahydroborate; In ethanol;

Reference yield:

: 97188-46-0
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-carboxylic acid pentafluorophenyl ester

: C₂₇H₃₃N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / NaBH₄ / ethanol / 1 h / 0 °C

2: 90 percent / triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

3: 83 percent / LiBr / acetone / 0.5 h / Heating

4: 2N NaOH, tetrabuthylammonium hydrogen sulfate / CH₂Cl₂ / 3 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; lithium bromide; In ethanol; dichloromethane; acetone;