1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

Base Information

Chemical Name:1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate
CAS No.:97188-52-8
Molecular Formula:C₁₇H₂₂NO₃
Molecular Weight:288.367
Hs Code.:

Synonyms:1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

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Technology Process of 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

There total 7 articles about 1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 98-88-4
benzoyl chloride

: 97188-48-2
1-oxyl-4-hydroxymethyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine

: 97188-52-8
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

Guidance literature:: With pyridine; at 5 ℃; for 3h;

Reference yield: 69.0%

: 532-32-1
sodium benzoate

: 97188-51-7
1-oxyl-4-bromomethyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine

: 97188-52-8
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 38632-29-0
1-Oxyl-1,2,5,6-tetrahydro-2,2,6,6-tetramethylpyridin-4-carboxylic acid radical

: 97188-52-8
1-oxyl-2,2,6,6-tetramethyl-1,2,5,6-tetrahydropyridine-4-yl methyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / dicyclohexylcarbodiimide / ethyl acetate / 3 h / Ambient temperature

2: 87 percent / NaBH₄ / ethanol / 1 h / 0 °C

3: 76 percent / pyridine / 3 h / 5 °C

With pyridine; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In ethanol; ethyl acetate;