1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-

Base Information

Chemical Name:1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-
CAS No.:115706-38-2
Molecular Formula:C₁₃H₁₅NO₄
Molecular Weight:249.266
Hs Code.:
Mol file:115706-38-2.mol

Synonyms:1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-

Suppliers and Price of 1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-

Chemical Property:

PSA：66.84000
LogP:1.51250

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo-

There total 2 articles about 1(2H)-Quinolineacetic acid, 3,4-dihydro-6-methoxy--alpha--methyl-2-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54197-66-9
3,4-dihydro-6-hydroxy-2(1H)-quinolinone

: 115706-38-2
2-(1,2,3,4-tetrahydro-2-oxo-6-methoxyquinolin-1-yl)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / potassium carbonate / dimethylformamide / Ambient temperature

2: 1.) NaH, 2.) aq. NaOH / 1.) toluene, 0 deg C, heating, 6 h, 2.) ethanol, heating, 45 min

With sodium hydroxide; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00119a008

Reference yield:

: 54197-64-7
6-methoxy-2-oxo-1,2,3,4-tetrahydroquinoline

: 535-11-5,41978-69-2
Ethyl 2-bromopropionate

: 115706-38-2
2-(1,2,3,4-tetrahydro-2-oxo-6-methoxyquinolin-1-yl)propionic acid

Guidance literature:: With sodium hydroxide; sodium hydride; Yield given. Multistep reaction; 1.) toluene, 0 deg C, heating, 6 h, 2.) ethanol, heating, 45 min;
DOI:10.1021/jm00119a008