[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

Base Information

Chemical Name:[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]
CAS No.:1381855-69-1
Molecular Formula:C₂₂H₁₆Cl₂N₂O₃
Molecular Weight:427.287
Hs Code.:

Synonyms:[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

Suppliers and Price of [4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

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Technology Process of [4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

There total 3 articles about [4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1381855-60-2
C₂₂H₁₇Cl₂NO₂

: 1381855-69-1
[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

Guidance literature:: With acetic acid; sodium nitrite; at 20 ℃;
DOI:10.1016/j.mencom.2012.05.020

Reference yield:

: 1338356-34-5
C₂₁H₁₅Cl₂NO₂

: 1381855-69-1
[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-ethane / 48.5 h / 0 - 20 °C

2: water; sodium hydroxide / ethanol / 1 h / 80 °C

3: acetic acid; sodium nitrite / 20 °C

With water; acetic acid; sodium hydroxide; sodium nitrite; In ethanol; 1,2-dichloro-ethane;
DOI:10.1016/j.mencom.2012.05.020

Reference yield:

: 1381855-51-1
C₂₂H₁₈Cl₂NO₂⁽¹⁺⁾*FO₃S^(1-)

: 1381855-69-1
[4-methyl-6-(N-methyl-N-nitrosoamino)-1,3-phenylene]bis[(4-chlorophenyl)methanone]

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / ethanol / 1 h / 80 °C

2: acetic acid; sodium nitrite / 20 °C

With water; acetic acid; sodium hydroxide; sodium nitrite; In ethanol;
DOI:10.1016/j.mencom.2012.05.020