(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

Base Information

Chemical Name:(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride
CAS No.:463342-82-7
Molecular Formula:C₁₄H₁₀Cl₃N₃O
Molecular Weight:342.612
Hs Code.:

Synonyms:(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

Chemical Property:

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Technology Process of (1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

There total 3 articles about (1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 31009-94-6
2-chloro-N-(3-chlorophenyl)-3-oxobutanamide

: 108-42-9
3-chloro-aniline

: 463342-82-7
(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

Guidance literature:: 3-chloro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

2-chloro-N-(3-chlorophenyl)-3-oxobutanamide; With sodium acetate; In methanol; water; at 5 - 10 ℃; for 2h; Further stages.;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U

Reference yield:

: 2415-87-4
3'-chloroacetoacetanilide

: 463342-82-7
(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: SO₂Cl₂ / toluene

2.1: HCl; sodium nitrite / H₂O / 0 - 5 °C

2.2: 72 percent / sodium acetate / methanol; H₂O / 2 h / 5 - 10 °C

With hydrogenchloride; sulfuryl dichloride; sodium nitrite; In water; toluene; 2.2: Japp-Klingemann reaction;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U

Reference yield:

: 108-42-9
3-chloro-aniline

: 463342-82-7
(1Z)-N-(3-chlorophenyl)-2-[(3-chlorophenyl)amino]-2-oxoethanehydrazonoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 150 - 160 °C

2.1: SO₂Cl₂ / toluene

3.1: HCl; sodium nitrite / H₂O / 0 - 5 °C

3.2: 72 percent / sodium acetate / methanol; H₂O / 2 h / 5 - 10 °C

With hydrogenchloride; sulfuryl dichloride; sodium nitrite; In water; toluene; 3.2: Japp-Klingemann reaction;
DOI:10.1002/1099-0690(200205)2002:10<1654::AID-EJOC1654>3.0.CO;2-U