Technology Process of C15H14O
There total 6 articles about C15H14O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium;
In
toluene;
at -78 - 20 ℃;
DOI:10.1021/ol2003308
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / acetonitrile / 20 °C / Inert atmosphere
2.1: Red-Al / tetrahydrofuran; toluene / 0 °C
2.2: -78 - 0 °C
3.1: pyridine; phosphorus tribromide / diethyl ether / 0 - 20 °C
4.1: N-benzyl-trimethylammonium hydroxide / methanol; water / 20 °C
5.1: pyridine / dichloromethane / -78 - 20 °C
6.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / toluene / -78 - 20 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; phosphorus tribromide; N-benzyl-trimethylammonium hydroxide; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ol2003308
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / -78 - 20 °C
2: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / toluene / -78 - 20 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium;
In
dichloromethane; toluene;
DOI:10.1021/ol2003308
