morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

Base Information

Chemical Name:morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid
CAS No.:87791-06-8
Molecular Formula:C₁₅H₂₁NO₄S₂
Molecular Weight:343.468
Hs Code.:

Synonyms:morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

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Chemical Property of morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

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Technology Process of morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

There total 1 articles about morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 74323-40-3
N-<(Z)-4-hydroxy-2-methylbut-2-ene-1-sulfonyl>morpholine

: 882-33-7
diphenyldisulfane

: 87791-06-8
morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

Guidance literature:: With n-butyllithium; 1.) THF-hexane, -40 deg C, 40 min, 2.) -35 deg C, 25 min; -> 10 deg C 1 h;
DOI:10.1007/BF00954348

Reference yield: 74.0%

: 87791-06-8
morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

: 556-82-1
3-methyl-2-buten-1-ol

Guidance literature:: With lithium; In ammonia; at -70 ℃; for 0.0833333h;
DOI:10.1007/BF00954348

Reference yield:

: 87791-06-8
morpholide of 1-phenylthio-4-hydroxy-2-methylbut-2Z-ene-1-sulfonic acid

: 106-25-2
Nerol

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 1.) n-BuLi, 2.) Li / 1.) THF-hexane, 0 deg C, 2.) NH₃ liq.m, -70 deg C, 5 min

2: 75 percent / 1.) n-BuLi / 1.) THF-hexane, -45 deg C, 40 min, 2.) -45 deg C, 40 min; -> 10 deg C 1 h

3: Li / diethyl ether; liquid ammonia / -65 °C / other reagent, solvent, temperature

With n-butyllithium; lithium; In diethyl ether; ammonia;
DOI:10.1007/BF00954348