benzhydrylidene aza-alaninyl-proline tert-butyl ester

Base Information

Chemical Name:benzhydrylidene aza-alaninyl-proline tert-butyl ester
CAS No.:1234782-90-1
Molecular Formula:C₂₄H₂₉N₃O₃
Molecular Weight:407.513
Hs Code.:

Synonyms:benzhydrylidene aza-alaninyl-proline tert-butyl ester

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Chemical Property of benzhydrylidene aza-alaninyl-proline tert-butyl ester

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Technology Process of benzhydrylidene aza-alaninyl-proline tert-butyl ester

There total 1 articles about benzhydrylidene aza-alaninyl-proline tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1234783-06-2
benzhydrylidene aza-glycinyl-proline tert-butyl ester

: 74-88-4
methyl iodide

: 1234782-90-1
benzhydrylidene aza-alaninyl-proline tert-butyl ester

Guidance literature:: benzhydrylidene aza-glycinyl-proline tert-butyl ester; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/psc.1235

Reference yield:

: 1234782-90-1
benzhydrylidene aza-alaninyl-proline tert-butyl ester

: 1234782-83-2
benzhydrylidene aza-alaninyl-proline diphenylmethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / dichloromethane / 2 h / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.08 h / -15 °C / Inert atmosphere

2.2: 2 h / -15 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/psc.1235