(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

Base Information

Chemical Name:(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate
CAS No.:1619923-56-6
Molecular Formula:C₂₃H₄₁N₂O₄PS
Molecular Weight:472.629
Hs Code.:

Synonyms:(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

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Chemical Property of (R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

Chemical Property:

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Technology Process of (R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

There total 3 articles about (R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1619923-54-4
(R)-(9H-fluoren-9-yl)methyl 4-oxo-1-(phenylthio)butan-2-ylcarbamate

: 1619923-55-5
di-tert-butyl piperidin-4-yl phosphate

: 1619923-56-6
(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

Guidance literature:: (R)-(9H-fluoren-9-yl)methyl 4-oxo-1-(phenylthio)butan-2-ylcarbamate; di-tert-butyl piperidin-4-yl phosphate; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;

With diethylamine; In acetonitrile; at 20 ℃;

Reference yield:

: 488761-06-4
C₂₄H₂₁NO₄S

: 1619923-56-6
(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 1 h / -10 °C / Inert atmosphere

1.2: 3 h / -10 - 20 °C

1.3: 1.25 h / -78 - -40 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

2.2: 20 °C

With sodium tris(acetoxy)borohydride; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 137348-86-8
di-tert-butyl diisopropylphosphoramide

: 351184-42-4
9H-fluoren-9-ylmethyl 4-hydroxy-1-piperidinecarboxylate

: 1619923-56-6
(R)-1-(3-amino-4-(phenylthio)butyl)piperidin-4-yl di-tert-butyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / acetonitrile; tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

2.2: 20 °C

With 1H-tetrazole; sodium tris(acetoxy)borohydride; In tetrahydrofuran; 1,2-dichloro-ethane; acetonitrile;