C₄₇H₆₀N₈O₆

Base Information

Chemical Name:C₄₇H₆₀N₈O₆
CAS No.:1419384-91-0
Molecular Formula:C₄₇H₆₀N₈O₆
Molecular Weight:833.043
Hs Code.:

C<sub>47</sub>H<sub>60</sub>N<sub>8</sub>O<sub>6</sub>

Synonyms:C₄₇H₆₀N₈O₆

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Chemical Property of C₄₇H₆₀N₈O₆

Chemical Property:

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Technology Process of C₄₇H₆₀N₈O₆

There total 12 articles about C₄₇H₆₀N₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: C₃₃H₃₈N₆*4ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1419384-91-0
C₄₇H₆₀N₈O₆

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 10h;

Reference yield:

: 13336-31-7
4-methoxylindanone

: 1419384-91-0
C₄₇H₆₀N₈O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice

2.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

3.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

4.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

7.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

7.2: 4 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C / Cooling with ice

9.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C / Sealed tube

10.1: hydrogenchloride / tetrahydrofuran; ethyl acetate / 10 h / 20 °C

11.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

With pyridine; hydrogenchloride; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; potassium tert-butylate; ammonium acetate; boron tribromide; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; toluene; acetonitrile;

Reference yield:

: 1419386-48-3
C₁₄H₁₆O₂

: 1419384-91-0
C₄₇H₆₀N₈O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 2 h / 20 °C

3.1: boron tribromide / dichloromethane / 24 h / -40 - 20 °C

4.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 90 °C

6.1: t-butyldimethylsiyl triflate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Cooling with ice

6.2: 4 h / 0 °C

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C / Cooling with ice

8.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 5 h / 140 °C / Sealed tube

9.1: hydrogenchloride / tetrahydrofuran; ethyl acetate / 10 h / 20 °C

10.1: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

With pyridine; hydrogenchloride; triethylsilane; aluminum (III) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butyldimethylsiyl triflate; ammonium acetate; boron tribromide; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetonitrile;