5,5-diphenyl-1,4,6,5-oxadithiastannocane

Base Information

• Chemical Name: 5,5-diphenyl-1,4,6,5-oxadithiastannocane
• CAS No.: 71573-72-3
• Molecular Formula: C₁₆H₁₈OS₂Sn
• Molecular Weight: 409.16
• Mol file: 71573-72-3.mol

Synonyms:5,5-diphenyl-1,4,6,5-oxadithiastannocane

Chemical Property of 5,5-diphenyl-1,4,6,5-oxadithiastannocane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 5,5-diphenyl-1,4,6,5-oxadithiastannocane

There total 2 articles about 5,5-diphenyl-1,4,6,5-oxadithiastannocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

diphenyltin(IV) dichloride (1135-99-5) + bis(2-mercaptoethyl)ether (2150-02-9) → [(2,2-oxydiethanethiolate)SnPh2] (71573-72-3)

Guidance literature:

With sodium ethanolate; In ethanol; benzene; for 10h; Inert atmosphere; Reflux;

DOI:10.2478/s11532-013-0250-3

Reference yield: 65.0%

diphenyltin(IV) dichloride (1135-99-5) + bis(2-mercaptoethyl)ether (2150-02-9) → 5,5-diphenyl-1,4,6,5-oxadithiastannocane (71573-72-3)

Guidance literature:

With Na; In ethanol; byproducts: NaCl; 1 h reflux of bis(2-mercaptoethyl) ether and Na in ethanol; slowly addn. Ph2SnCl2/benzene soln.; 4 h reflux; NaCl warm filtered; concd.; cooled; filtered; recrystd. from ethanol.; elem. anal.;

upstream raw materials:

diphenyltin(IV) dichloride

bis(2-mercaptoethyl)ether