5,5-diphenyl-1,4,6,5-oxadithiastannocane

Base Information

Chemical Name:5,5-diphenyl-1,4,6,5-oxadithiastannocane
CAS No.:71573-72-3
Molecular Formula:C₁₆H₁₈OS₂Sn
Molecular Weight:409.16
Hs Code.:

Synonyms:5,5-diphenyl-1,4,6,5-oxadithiastannocane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5-diphenyl-1,4,6,5-oxadithiastannocane

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Technology Process of 5,5-diphenyl-1,4,6,5-oxadithiastannocane

There total 2 articles about 5,5-diphenyl-1,4,6,5-oxadithiastannocane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1135-99-5
diphenyltin(IV) dichloride

: 2150-02-9
bis(2-mercaptoethyl)ether

: 71573-72-3
[(2,2-oxydiethanethiolate)SnPh₂]

Guidance literature:: With sodium ethanolate; In ethanol; benzene; for 10h; Inert atmosphere; Reflux;
DOI:10.2478/s11532-013-0250-3

Reference yield: 65.0%

: 1135-99-5
diphenyltin(IV) dichloride

: 2150-02-9
bis(2-mercaptoethyl)ether

: 71573-72-3
5,5-diphenyl-1,4,6,5-oxadithiastannocane

Guidance literature:: With Na; In ethanol; byproducts: NaCl; 1 h reflux of bis(2-mercaptoethyl) ether and Na in ethanol; slowly addn. Ph2SnCl2/benzene soln.; 4 h reflux; NaCl warm filtered; concd.; cooled; filtered; recrystd. from ethanol.; elem. anal.;