11-phenylbenzofluorene

Base Information

• Chemical Name: 11-phenylbenzo
• Molecular Formula: C₂₃H₁₆
• Molecular Weight: 292.38

Synonyms:11-phenylbenzofluorene

Chemical Property of 11-phenylbenzo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 21 articles about 11-phenylbenzofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1-(1-methoxy-3-phenylprop-2-yn-1-yl)-2-(phenylethynyl)benzene (1215270-29-3) → 11-phenylbenzofluorene (104601-29-8)

Guidance literature:

1-(1-methoxy-3-phenylprop-2-yn-1-yl)-2-(phenylethynyl)benzene; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 14h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 3h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;

DOI:10.1021/ja510563d

Reference yield: 86.0%

tributyl(11-phenyl-11H-benzo[a]-fluoren-6-yl)stannane → 11-phenylbenzofluorene (104601-29-8)

Guidance literature:

With hydrogenchloride; In dichloromethane; water; for 3h; Inert atmosphere;

DOI:10.1021/ja510563d

Reference yield: 72.0%

3-phenyl-1-(2-(phenylethynyl)phenyl)-prop-2-yn-1-ol (216306-60-4) → 11-phenylbenzofluorene (104601-29-8)

Guidance literature:

3-phenyl-1-(2-(phenylethynyl)phenyl)-prop-2-yn-1-ol; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 30h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 3h; Inert atmosphere;

DOI:10.1021/ja510563d

upstream raw materials:

naphthalene

Dichlorodiphenylmethane

1-naphthyldiphenylmethanol

1-(chlorodiphenylmethyl)naphthalene

Downstream raw materials:

Diphenylacetonitrile

2-Benzoylbenzoic acid

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