benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

Base Information

Chemical Name:benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate
CAS No.:309743-80-4
Molecular Formula:C₂₅H₂₅NO₅
Molecular Weight:419.477
Hs Code.:

Synonyms:benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

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Chemical Property of benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

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Technology Process of benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

There total 1 articles about benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 98-88-4
benzoyl chloride

: 68781-38-4
benzyl 3-(2-ethoxycarbonylethyl)-4-methylpyrrole-2-carboxylate

: 309743-80-4
benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 0 - 20 ℃; for 3.75h;

Reference yield: 79.0%

: 309743-80-4
benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

: 309743-67-7
benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-(1-hydroxybenzyl)pyrrole-2-carboxylate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 309743-80-4
benzyl 3-(2-ethoxycarbonylethyl)-4-methyl-5-benzoylpyrrole-2-carboxylate

: 2-(2-acetoxyethyl)-8-(2-ethoxycarbonylethyl)-3,7,13,14-tetramethyl-12-(2-methoxycarbonylethyl)-1-tert-butoxycarbonyl-5-phenyl-5,17-dihydrotripyrrin hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / NaBH₄ / methanol; CH₂Cl₂ / 0.5 h / 20 °C

2: 99 percent / p-toluenesulfonic acid / CH₂Cl₂ / 1 h / 20 °C

3: 66 percent / H₂ / 10 percent Pd/C / ethanol / 3 h / 2585.74 Torr

4: 94 percent / p-toluenesulfonic acid; HBr(g) / CH₂Cl₂; methanol / 1 h / 20 °C

With sodium tetrahydroborate; hydrogen bromide; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; dichloromethane;