Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

Base Information Edit

Chemical Name:Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)
CAS No.:115378-33-1
Molecular Formula:C9H17 N O2
Molecular Weight:171.239
Hs Code.:
Mol file:115378-33-1.mol

Synonyms:Carbamicacid, (1-methyl-2-propenyl)-, 1,1-dimethylethyl ester, (S)-; Carbamic acid, [(1S)-1-methyl-2-propenyl]-,1,1-dimethylethyl ester (9CI); (S)-3-[(tert-Butoxycarbonyl)amino]-1-butene;tert-Butyl ((1S)-1-methylprop-2-enyl)carbamate

Suppliers and Price of Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI) Edit

Chemical Property:

PSA：38.33000
LogP:2.47650

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

There total 10 articles about Carbamic acid, [(1S)-1-methyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 129076-07-9
(-)-di-tert-butyl [(1S)-1-methylprop-2-en-1-yl]imidodicarbonate

: 115378-33-1
(-)-tert-butyl [(1S)-1-methylprop-2-en-1-yl]carbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1002/ejoc.201501333

Reference yield: 86.0%

: 1033286-96-2
(S)-tert-butyl formyl(1-methylprop-2-en-1-yl)carbamate

: 115378-33-1
(-)-tert-butyl [(1S)-1-methylprop-2-en-1-yl]carbamate

Guidance literature:: With potassium hydroxide; In methanol;
DOI:10.1055/s-2008-1042899

Reference yield: 82.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 79069-50-4
Boc-Ala-H

: 115378-33-1
(-)-tert-butyl [(1S)-1-methylprop-2-en-1-yl]carbamate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

Boc-Ala-H; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1021/acsmedchemlett.0c00572