C₃₉H₄₈N₂O₇SSi

Base Information

Chemical Name:C₃₉H₄₈N₂O₇SSi
CAS No.:1352230-48-8
Molecular Formula:C₃₉H₄₈N₂O₇SSi
Molecular Weight:716.971
Hs Code.:

C<sub>39</sub>H<sub>48</sub>N<sub>2</sub>O<sub>7</sub>SSi

Synonyms:C₃₉H₄₈N₂O₇SSi

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Chemical Property of C₃₉H₄₈N₂O₇SSi

Chemical Property:

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Technology Process of C₃₉H₄₈N₂O₇SSi

There total 20 articles about C₃₉H₄₈N₂O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 994-30-9
triethylsilyl chloride

: 1352230-46-6
C₃₃H₃₄N₂O₇S

: 1352230-48-8
C₃₉H₄₈N₂O₇SSi

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1352230-48-8
C₃₉H₄₈N₂O₇SSi

Guidance literature:: Multi-step reaction with 14 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

4.2: 3 h / -78 °C

4.3: 20 °C

5.1: sulfuric acid / 2 h / 20 °C

6.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

6.2: 0 - 60 °C

7.1: potassium carbonate / methanol / 96 h / 20 °C

7.2: 12 h / 0 °C

8.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

8.2: 1.5 h

9.1: pyridine / 5.5 h / 0 - 20 °C

10.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

10.2: 12 h

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

13.1: pyridine / 6.5 h / 0 - 20 °C

14.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

With pyridine; 1H-imidazole; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 1352230-48-8
C₃₉H₄₈N₂O₇SSi

Guidance literature:: Multi-step reaction with 17 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 1 h / -78 - 20 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

7.2: 3 h / -78 °C

7.3: 20 °C

8.1: sulfuric acid / 2 h / 20 °C

9.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

9.2: 0 - 60 °C

10.1: potassium carbonate / methanol / 96 h / 20 °C

10.2: 12 h / 0 °C

11.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

11.2: 1.5 h

12.1: pyridine / 5.5 h / 0 - 20 °C

13.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

13.2: 12 h

14.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

16.1: pyridine / 6.5 h / 0 - 20 °C

17.1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

With pyridine; 1H-imidazole; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;