(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

Base Information

Chemical Name:(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol
CAS No.:1025510-61-5
Molecular Formula:C₃₃H₆₆O₆Si₃
Molecular Weight:643.14
Hs Code.:

Synonyms:(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

Chemical Property:

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Technology Process of (+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

There total 2 articles about (+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-methyl-3-triethylsiloxybutylmagnesium bromide

: 1073897-00-3
C₂₂H₄₀O₅Si₂

: 1025510-62-6
(+)-2-(1-hydroxy-5-triethylsilyloxy-1,5-dimethylhexyl)-5-(2-trimethylsilylethoxymethoxymethyl)phenol

: 1025510-61-5
(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; at -10 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.02.094

Reference yield:

: 1073897-00-3
C₂₂H₄₀O₅Si₂

: 87417-12-7
(3-bromo-1,1-dimethylpropoxy)triethylsilane

: 1025510-62-6
(+)-2-(1-hydroxy-5-triethylsilyloxy-1,5-dimethylhexyl)-5-(2-trimethylsilylethoxymethoxymethyl)phenol

: 1025510-61-5
(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

Guidance literature:: (3-bromo-1,1-dimethylpropoxy)triethylsilane; With iodine; magnesium; In diethyl ether; for 2h;

With copper(l) iodide; In tetrahydrofuran; diethyl ether; at -10 ℃; for 0.5h;

C₂₂H₄₀O₅Si₂; In tetrahydrofuran; diethyl ether; at -10 ℃; for 1h;
DOI:10.1016/j.tet.2008.08.012

Reference yield: 80.0%

: 1025510-61-5
(+)-6-triethylsilyloxy-6-methyl-2-[2-(2-trimethylsilylethoxymethoxy)-4-(2-trimethylsilylethoxymethoxymethyl)phenyl]heptan-2-ol

: 848645-02-3
(+)-curcutetraol

Guidance literature:: With molecular sieve; tetrabutyl ammonium fluoride; In tetrahydrofuran; for 5h; Heating;
DOI:10.1016/j.tetlet.2008.02.094