methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

Base Information

Chemical Name:methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate
CAS No.:338465-86-4
Molecular Formula:C₁₆H₂₆N₂S₂
Molecular Weight:310.528
Hs Code.:

Synonyms:methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

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Chemical Property of methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

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Technology Process of methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

There total 1 articles about methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 20184-94-5
N-methyl-hydrazinecarbodithioic acid methyl ester

: 96843-20-8
5-cyclohexylidene-3,3-dimethylpent-4-en-2-one

: 338465-86-4
methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

Guidance literature:: With 4 A molecular sieve; toluene-4-sulfonic acid; In toluene; for 16h; Heating;
DOI:10.1002/1099-0690(200103)2001:5<941::AID-EJOC941>3.0.CO;2-E

Reference yield:

: 338465-86-4
methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

: 468095-31-0
5-cyclohexyl-2,3,3-trimethyl-pyrrolidine

Guidance literature:: methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate; With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In cyclohexane; for 5h; Heating;

With sodium tetrahydroborate; benzoic acid; In tetrahydrofuran; at 20 ℃; for 3h; Further stages.;
DOI:10.1002/1099-0690(200103)2001:5<941::AID-EJOC941>3.0.CO;2-E

Reference yield:

: 338465-86-4
methyl 2-(4-cyclohexylidene-1,2,2-trimethyl-3-butenylidene)-1-methylhydrazine carbodithioate

: 1-benzoyl-5-cyclohexyl-2,3,3-trimethylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: AIBN; Bu₃SnH / cyclohexane / 5 h / Heating

1.2: NaBH₄; PhCO₂H / tetrahydrofuran / 3 h / 20 °C

2.1: pyridine / diethyl ether / 3 h

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In diethyl ether; cyclohexane;
DOI:10.1002/1099-0690(200103)2001:5<941::AID-EJOC941>3.0.CO;2-E