4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

Base Information

Chemical Name:4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate
CAS No.:1440200-15-6
Molecular Formula:C₂₉H₃₀BrN₃O₄
Molecular Weight:564.479
Hs Code.:

Synonyms:4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

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Chemical Property of 4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

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Technology Process of 4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

There total 2 articles about 4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1440200-03-2
(R)-4-[1-(4-bromophenyl)-2-nitroethyl]-5-methyl-2-phenyl-2H-pyrazol-3-ol

: 2094-72-6
1-Adamantanecarbonyl chloride

: 1440200-15-6
4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

Guidance literature:: With triphenylphosphine; In dichloromethane; at 20 ℃;
DOI:10.1002/chem.201202636

Reference yield:

: 89-25-8
edaravone

: 1440200-15-6
4-(1-(4-bromophenyl)-2-nitroethyl)-3-methyl-1-phenyl-1H-pyrazol-5-adamantane carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: C₃₁H₃₉N₃O₉S; benzoic acid / toluene / 20 °C / Inert atmosphere

2: triphenylphosphine / dichloromethane / 20 °C

With C₃₁H₃₉N₃O₉S; triphenylphosphine; benzoic acid; In dichloromethane; toluene;
DOI:10.1002/chem.201202636