C₃₁H₃₉IO₃Si

Base Information

Chemical Name:C₃₁H₃₉IO₃Si
CAS No.:1365694-05-8
Molecular Formula:C₃₁H₃₉IO₃Si
Molecular Weight:614.639
Hs Code.:

C<sub>31</sub>H<sub>39</sub>IO<sub>3</sub>Si

Synonyms:C₃₁H₃₉IO₃Si

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Chemical Property of C₃₁H₃₉IO₃Si

Chemical Property:

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Technology Process of C₃₁H₃₉IO₃Si

There total 11 articles about C₃₁H₃₉IO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75-47-8
iodoform

: 1365694-15-0
C₃₀H₃₈O₄Si

: 1365694-05-8
C₃₁H₃₉IO₃Si

Guidance literature:: With chromium dichloride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.tetlet.2012.01.032

Reference yield:

: 5390-04-5
pent-1-yn-5-ol

: 1365694-05-8
C₃₁H₃₉IO₃Si

Guidance literature:: Multi-step reaction with 8 steps

2: toluene-4-sulfonic acid

3: copper(l) iodide; potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 20 °C

4: methanol / dichloromethane / 20 °C

5: quinoline; hydrogen / ethyl acetate / 20 °C

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

7: toluene / 2 h / Reflux

8: chromium dichloride / tetrahydrofuran / 0 °C

With quinoline; chromium dichloride; methanol; copper(l) iodide; oxalyl dichloride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; 1: Jones oxidation / 5: Lindlar hydrogenation / 6: Swern oxidation / 7: Wittig homologation / 8: Takai olefination;
DOI:10.1016/j.tetlet.2012.01.032

Reference yield:

: 6089-09-4
4-pentynoic acid

: 1365694-05-8
C₃₁H₃₉IO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1: toluene-4-sulfonic acid

2: copper(l) iodide; potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 20 °C

3: methanol / dichloromethane / 20 °C

4: quinoline; hydrogen / ethyl acetate / 20 °C

5: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

6: toluene / 2 h / Reflux

7: chromium dichloride / tetrahydrofuran / 0 °C

With quinoline; chromium dichloride; methanol; copper(l) iodide; oxalyl dichloride; hydrogen; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; 4: Lindlar hydrogenation / 5: Swern oxidation / 6: Wittig homologation / 7: Takai olefination;
DOI:10.1016/j.tetlet.2012.01.032