Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI)

Base Information

• Chemical Name: Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI)
• CAS No.: 115012-02-7
• Molecular Formula: C₆H₉N₃O₃
• Molecular Weight: 171.156
• Mol file: 115012-02-7.mol

Synonyms:Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI)

Chemical Property of Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI)

Chemical Property:

• Melting Point: 132-133 °C(Solv: ethyl acetate (141-78-6); ethyl ether (60-29-7))
• PKA: 7.12±0.20(Predicted)
• Density: 1.42±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI)

There total 1 articles about Carbamic acid, (4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl)-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Creatinine (60-27-5) + 1-methoxycarbonyl-3-methylimidazolium chloride → 2-methoxycarbonylamino-1-methyl-1,5-dihydro-4H-imidazol-4-one (115012-02-7)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 2h; Yield given;

DOI:10.1246/bcsj.60.4115

Reference yield: 80.0%

2-methoxycarbonylamino-1-methyl-1,5-dihydro-4H-imidazol-4-one (115012-02-7) → 2-methoxycarbonylamino-1-methyl-1H-imidazole-4,5-dione

Guidance literature:

With mercury(II) diacetate; In chloroform; water; at 20 ℃; for 1.5h; under the protection of light;

DOI:10.1246/bcsj.60.4115

upstream raw materials:

Creatinine

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