Technology Process of C15H21N3O2S2
There total 6 articles about C15H21N3O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Thioctic acid;
With
pyridine; 1,1'-carbonyldiimidazole;
In
N,N-dimethyl-formamide;
at 45 ℃;
for 0.5h;
3-carbamoylbenzene-1,2-diaminium dichloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium hydroxide
2.1: potassium hydroxide; bromine / Heating
3.1: thionyl chloride
4.1: Raney nickel / ethyl acetate; ethanol
5.1: pyridine; 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 0.5 h / 45 °C
5.2: 20 °C
With
pyridine; ammonium hydroxide; thionyl chloride; bromine; 1,1'-carbonyldiimidazole; potassium hydroxide;
Raney nickel;
In
ethanol; ethyl acetate; N,N-dimethyl-formamide;
2.1: Hofmann Rearrangement;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Raney nickel / ethyl acetate; ethanol
2.1: pyridine; 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 0.5 h / 45 °C
2.2: 20 °C
With
pyridine; 1,1'-carbonyldiimidazole;
Raney nickel;
In
ethanol; ethyl acetate; N,N-dimethyl-formamide;