cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

Base Information

Chemical Name:cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene
CAS No.:1416572-98-9
Molecular Formula:C₆₉H₈₁N₉O₉
Molecular Weight:1180.46
Hs Code.:

Synonyms:cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

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Chemical Property of cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

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Technology Process of cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

There total 2 articles about cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1263293-78-2
7,15,23-tri-tert-butyl-25,26,27-tris(propargyloxy)hexahomotrioxacalix[3]arene

: 70978-37-9
1-(azidomethyl)-4-methoxybenzene

: 1416572-98-9
cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; water; at 50 ℃; for 24h;
DOI:10.1039/c2nj40599g

Reference yield:

: 76543-12-9
p-(tert-butyl)hexahomotrioxacalix[3]arene

: 1416572-98-9
cone-7,15,23-tri-tert-butyl-25,26,27-tris{[1H-(4-methoxybenzyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3]arene

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / acetone / 1 h / Reflux

1.2: 18 h / Reflux

2.1: copper(l) iodide / tetrahydrofuran; water / 24 h / 50 °C

With copper(l) iodide; caesium carbonate; In tetrahydrofuran; water; acetone;
DOI:10.1039/c2nj40599g