C₂₂H₂₀O₃

Base Information

Chemical Name:C₂₂H₂₀O₃
CAS No.:1579264-53-1
Molecular Formula:C₂₂H₂₀O₃
Molecular Weight:332.399
Hs Code.:

C<sub>22</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₀O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₀O₃

Chemical Property:

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Technology Process of C₂₂H₂₀O₃

There total 3 articles about C₂₂H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 696-62-8
para-iodoanisole

: 110598-51-1
2-(1-(4-methoxyphenyl)vinyl)phenol

: 1579264-53-1
C₂₂H₂₀O₃

Guidance literature:: With palladium diacetate; potassium carbonate; Trimethylacetic acid; In N,N-dimethyl acetamide; at 160 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc49717h

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 1579264-53-1
C₂₂H₂₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 8 h / 0 °C / Reflux

1.2: Reflux

2.1: potassium carbonate; palladium diacetate; Trimethylacetic acid / N,N-dimethyl acetamide / 1 h / 160 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; Trimethylacetic acid; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1039/c3cc49717h

Reference yield:

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 1579264-53-1
C₂₂H₂₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 8 h / 0 °C / Reflux

1.2: Reflux

2.1: potassium carbonate; palladium diacetate; Trimethylacetic acid / N,N-dimethyl acetamide / 1 h / 160 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; Trimethylacetic acid; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1039/c3cc49717h