3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

Base Information Edit

Chemical Name:3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester
CAS No.:632352-54-6
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:
Mol file:632352-54-6.mol

Synonyms:3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

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Chemical Property of 3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

There total 5 articles about 3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76041-06-0
ethyl 3-[(2-ethoxycarbonyl)ethylamino]-2-phenylpropionate

: 100-39-0
benzyl bromide

: 632352-54-6
3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

Guidance literature:: With sodium carbonate; In acetonitrile; at 75 ℃; for 2h;

Reference yield:

: 22319-48-8
ethyl 2-phenyl-3-(N-benzylamino)propionate

: 140-88-5,9003-32-1
ethyl acrylate

: 632352-54-6
3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

Guidance literature:: With acetic acid; for 12h; Heating / reflux;

Reference yield:

: 101-97-3
Ethyl 2-phenylethanoate

: 632352-54-6
3-[benzyl-(2-ethoxycarbonyl-ethyl)-amino]-2-phenyl-propionic acid ethy ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; sodium hydride; oxalic acid diethyl ester / 5,5-dimethyl-1,3-cyclohexadiene; mineral oil / 14 h / 0 - 20 °C

1.2: 1 h

1.3: 14 h

2.1: triethylamine / 18 h / 20 °C

3.1: sodium carbonate / acetonitrile / 2 h / 70 °C

With ethanol; sodium hydride; sodium carbonate; triethylamine; oxalic acid diethyl ester; In 5,5-dimethyl-1,3-cyclohexadiene; acetonitrile; mineral oil; 2.1: Michael addition;
DOI:10.1016/j.bmc.2011.08.070