(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

Base Information

Chemical Name:(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one
CAS No.:202932-15-8
Molecular Formula:C₂₅H₂₃NO₄
Molecular Weight:401.462
Hs Code.:

Synonyms:(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

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Technology Process of (4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

There total 1 articles about (4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 16251-45-9,17097-67-5,28044-22-6,28044-23-7,39663-75-7,54418-69-8,77943-39-6,125133-96-2,149055-02-7
(4S,5R)-4-methyl-5-phenyl-oxazolidin-2-one

: 39188-62-0
2-(4-(benzyloxy)phenyl)acetyl chloride

: 202932-15-8
(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;
DOI:10.1039/a706163c

Reference yield: 59.0%

: 125453-11-4
benzyl N-(1H-benzotriazol-1-ylmethyl)carbamate

: 202932-15-8
(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

: [(S)-2-(4-Benzyloxy-phenyl)-3-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid benzyl ester

: 202932-27-2
[(R)-2-(4-Benzyloxy-phenyl)-3-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid benzyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -60 - 8 ℃; for 3h;
DOI:10.1039/a706163c

Reference yield: 56.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 202932-15-8
(4S,5R)-3-[2-(4-Benzyloxy-phenyl)-acetyl]-4-methyl-5-phenyl-oxazolidin-2-one

: (R)-3-(4-Benzyloxy-phenyl)-4-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-4-oxo-butyric acid tert-butyl ester

: 202932-21-6
(S)-3-(4-Benzyloxy-phenyl)-4-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-4-oxo-butyric acid tert-butyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; Yield given. Title compound not separated from byproducts; 1.) -72 deg C, 30 min, 2.) -72 to -20 deg C, 2 h;
DOI:10.1039/a706163c