N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

Base Information

Chemical Name:N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide
CAS No.:87438-04-8
Molecular Formula:C₁₇H₂₅N₃O₄
Molecular Weight:335.403
Hs Code.:

Synonyms:N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

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Chemical Property of N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

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Technology Process of N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

There total 4 articles about N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 96866-13-6
N-(benzyloxy)-N-formyl-L-phenylalanylglycine isopentylamide

: 87438-04-8
N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 42990-55-6,35016-63-8,42990-49-8,16503-53-0
(S)-(alpha)-bromobenzenepropanoic acid

: 87438-04-8
N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

Guidance literature:: Multi-step reaction with 4 steps

1: 23 percent / methanol / Heating

2: 91 percent / acetic anhydride / 3 h / 0 °C

3: 85 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

4: 88 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 96866-10-3
N-benzyloxy-L-phenylalanine

: 87438-04-8
N-formyl-N-hydroxy-L-phenylalanylglycine isopentyl amide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / acetic anhydride / 3 h / 0 °C

2: 85 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

3: 88 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007