2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 81098-36-4
• Molecular Formula: C₁₆H₁₅F₁₅N₃O₅P₃
• Molecular Weight: 707.21

Synonyms:2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

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Technology Process of 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 3 articles about 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,1'-diphenyl-3,3,3',3',5,5,5',5'-octachlorobi(cyclotriphosphazene) (21229-71-0) + sodium 2,2,2-trifluoroethanolate (420-87-1) → 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-36-4)

Guidance literature:

In tetrahydrofuran; tetrachloromethane; at 24 ℃; for 24h;

DOI:10.1021/ja00373a024

Reference yield:

P(C6H5)(P(C6H5)2Fe(CO)4)NP(Cl)2NP(Cl)2N (124716-29-6) → 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-36-4)

Guidance literature:

With NaOCH₂CF₃; In tetrahydrofuran; under dry Ar; soln. of NaOCH2CF3 prepared, filtered, added to soln. of P.-compd. at 25°C, formation of intermediate after 2h, formation of endproduct after 24h; addn. of SiMe3Cl, solvent removed, extd. (CH2Cl2), filtered (silica gel), concd., diluted with hexane, volume reduced, cooled to -55°C;

Reference yield:

diphenyl(2-phenyl-4,4,6,6-tetrachloro-2-cyclotriphosphazenyl)phosphine-P (124716-24-1) → 2-Phenyl-2,4,4,6,6-pentakis-(2,2,2-trifluoro-ethoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-36-4)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: NaOCH₂CF₃ / tetrahydrofuran

With NaOCH₂CF₃; In tetrahydrofuran; toluene;

upstream raw materials:

1,1'-diphenyl-3,3,3',3',5,5,5',5'-octachlorobi(cyclotriphosphazene)

sodium 2,2,2-trifluoroethanolate

P(C₆H₅)(P(C₆H₅)2Fe(CO)4)NP(Cl)2NP(Cl)2N

diphenyl(2-phenyl-4,4,6,6-tetrachloro-2-cyclotriphosphazenyl)phosphine-P

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