(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

Base Information

Chemical Name:(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide
CAS No.:1459793-13-5
Molecular Formula:C₁₉H₂₈INOS
Molecular Weight:445.408
Hs Code.:

Synonyms:(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

Chemical Property:

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Technology Process of (S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

There total 5 articles about (S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 934016-05-4
3-[(1-iodomethyl)cyclohexyl]propanal

: 607729-50-0
(S)-(+)-2,4,6-trimethylbenzenesulfinamide

: 1459793-13-5
(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c3cc45452e

Reference yield:

: 3289-28-9
ethyl cyclohexanecarboxylate

: 1459793-13-5
(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

3.1: 1H-imidazole; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: osmium(VIII) oxide; water / 1,4-dioxane / 0.5 h / 20 °C

4.2: 2 h / 20 °C

5.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) tetraethanolate; osmium(VIII) oxide; water; diisobutylaluminium hydride; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;
DOI:10.1039/c3cc45452e

Reference yield:

: 934016-15-6
1-(but-3-en-1-yl)-1-(iodomethyl)cyclohexane

: 1459793-13-5
(S)-N-(3-(1-(iodomethyl)cyclohexyl)propylidene)-2,4,6-trimethylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: osmium(VIII) oxide; water / 1,4-dioxane / 0.5 h / 20 °C

1.2: 2 h / 20 °C

2.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; osmium(VIII) oxide; water; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c3cc45452e