1,1-dimethoxy-2-phenylselenenylhexane

Base Information

Chemical Name:1,1-dimethoxy-2-phenylselenenylhexane
CAS No.:266683-61-8
Molecular Formula:C₁₄H₂₂O₂Se
Molecular Weight:301.287
Hs Code.:

Synonyms:1,1-dimethoxy-2-phenylselenenylhexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-dimethoxy-2-phenylselenenylhexane

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Technology Process of 1,1-dimethoxy-2-phenylselenenylhexane

There total 2 articles about 1,1-dimethoxy-2-phenylselenenylhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 18207-17-5
α-bromohexanal dimethylacetal

: 1666-13-3
diphenyl diselenide

: 266683-61-8
1,1-dimethoxy-2-phenylselenenylhexane

Guidance literature:: With potassium carbonate; hydrazine hydrate; In dimethyl sulfoxide; at 70 ℃; for 7h;
DOI:10.1021/jo9917644

Reference yield:

: 1599-47-9
1,1-dimethoxyhexane

: 266683-61-8
1,1-dimethoxy-2-phenylselenenylhexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Br₂ / CH₂Cl₂ / 25 - 30 °C

1.2: 83 percent / 0.05 h

2.1: 84 percent / K₂CO₃; N₂H₄*H₂O / dimethylsulfoxide / 7 h / 70 °C

With bromine; potassium carbonate; hydrazine hydrate; In dichloromethane; dimethyl sulfoxide; 1.1: Bromination / 1.2: alcoholysis / 2.1: Substitution;
DOI:10.1021/jo9917644

Reference yield:

: 266683-61-8
1,1-dimethoxy-2-phenylselenenylhexane

: 18318-83-7
(E)-1,1-dimethoxy-2-hexene

: (Z)-1,1-dimethoxy-2-hexene

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 5h; Title compound not separated from byproducts.;
DOI:10.1021/jo9917644