4-<(benzyloxycarbonyl)amino>cycloheptanone

Base Information

Chemical Name:4-<(benzyloxycarbonyl)amino>cycloheptanone
CAS No.:142010-00-2
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:

Synonyms:4-<(benzyloxycarbonyl)amino>cycloheptanone

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Chemical Property of 4-<(benzyloxycarbonyl)amino>cycloheptanone

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Technology Process of 4-<(benzyloxycarbonyl)amino>cycloheptanone

There total 3 articles about 4-<(benzyloxycarbonyl)amino>cycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 95798-92-8
cis-4-(<(benzyloxy)carbonyl>amino)cycloheptanol

: 142010-00-2
4-<(benzyloxycarbonyl)amino>cycloheptanone

Guidance literature:: With chromic acid; In various solvent(s); Ambient temperature;
DOI:10.1039/P19940002559

Reference yield:

: 146309-04-8
6-Oxa-7-aza-bicyclo[3.2.2]non-8-ene-7-carboxylic acid benzyl ester

: 142010-00-2
4-<(benzyloxycarbonyl)amino>cycloheptanone

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / potassium azodicarboxylate, glacial ethanoic acid / methanol / 2 h / Ambient temperature

2: 98 percent / sodium amalgam / ethanol / 1 h / 0 °C / buffered with sodium phosphate

3: 96 percent / chromic acid / various solvent(s) / Ambient temperature

With sodium amalgam; potassium diazodicarboxylate; chromic acid; acetic acid; In methanol; ethanol;
DOI:10.1039/P19940002559

Reference yield:

: 159022-56-7
benzyl 8-oxa-9-azabicyclo<3.2.2>nonane-9-carboxylate

: 142010-00-2
4-<(benzyloxycarbonyl)amino>cycloheptanone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium amalgam / ethanol / 1 h / 0 °C / buffered with sodium phosphate

2: 96 percent / chromic acid / various solvent(s) / Ambient temperature

With sodium amalgam; chromic acid; In ethanol;
DOI:10.1039/P19940002559