p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:1206791-32-3
Molecular Formula:C₂₇H₂₄ClNO₆S
Molecular Weight:526.01
Hs Code.:

Synonyms:p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Chemical Property of p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.3%

: 1206791-33-4
p-chlorophenyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 100-39-0
benzyl bromide

: 1206791-32-3
p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: p-chlorophenyl 2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; With di(n-butyl)tin oxide; In toluene; at 80 ℃;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In toluene; at 80 ℃; for 24h; regioselective reaction;
DOI:10.1039/b914193f

Reference yield: 85.0%

: 1206791-32-3
p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 146292-90-2
6-azidohexan-1-ol

: 1206791-36-7
6-azidohexyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; 6-azidohexan-1-ol; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Molecular sieve;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -78 - -10 ℃; for 1h; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -78 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1039/b914193f

Reference yield: 52.0%

: 1206791-32-3
p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: O-(2,3,4-tri-O-benzyl-α/β-L-fucopyranosyl) trichloroacetimidate

: 1206791-53-8
p-chlorophenyl 2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1206791-54-9
p-chlorophenyl 2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->4)-6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: p-chlorophenyl 6-O-benzyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside; O-(2,3,4-tri-O-benzyl-α/β-L-fucopyranosyl) trichloroacetimidate; In dichloromethane; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1039/b914193f