C₁₈H₂₉FO₃SSi

Base Information

Chemical Name:C₁₈H₂₉FO₃SSi
CAS No.:1338560-74-9
Molecular Formula:C₁₈H₂₉FO₃SSi
Molecular Weight:372.576
Hs Code.:

C<sub>18</sub>H<sub>29</sub>FO<sub>3</sub>SSi

Synonyms:C₁₈H₂₉FO₃SSi

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Chemical Property of C₁₈H₂₉FO₃SSi

Chemical Property:

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Technology Process of C₁₈H₂₉FO₃SSi

There total 4 articles about C₁₈H₂₉FO₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17277-58-6
methyl (phenylsulfanyl)acetate

: 1338560-73-8
C₁₀H₂₀F₄O₄SSi

: 1338560-74-9
C₁₈H₂₉FO₃SSi

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; optical yield given as %de;
DOI:10.1016/j.bmcl.2011.08.011

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1338560-74-9
C₁₈H₂₉FO₃SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane / 0 °C

3: 2,6-dimethylpyridine / dichloromethane / 0 °C

4: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.08.011

Reference yield:

: 1338560-71-6
C₁₅H₃₅FO₂Si₂

: 1338560-74-9
C₁₈H₂₉FO₃SSi

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol; dichloromethane / 0 °C

2: 2,6-dimethylpyridine / dichloromethane / 0 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.08.011