N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide

Base Information

• Chemical Name: N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide
• CAS No.: 890662-14-3
• Molecular Formula: C₁₁H₁₅NO₃S
• Molecular Weight: 241.311
• Mol file: 890662-14-3.mol

Synonyms:N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide

Chemical Property of N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

N,4-Dimethyl-N-(oxiran-2-ylmethyl)-benzenesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide

There total 3 articles about N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,2-Epoxy-3-bromopropane (3132-64-7,82584-73-4) + N-methyl-p-toluenesulfonylamide (640-61-9) → N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide (890662-14-3)

Guidance literature:

N-methyl-p-toluenesulfonylamide; With sodium hydride; In tetrahydrofuran; mineral oil; Inert atmosphere;

1,2-Epoxy-3-bromopropane; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; for 16h; Inert atmosphere;

DOI:10.1039/c1ob06569f

Reference yield:

N-allyl-N-methyl-4-toluene sulphonamide (112497-43-5) → N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide (890662-14-3)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Product distribution / selectivity;

Reference yield:

epichlorohydrin (106-89-8,24969-06-0,13403-37-7) + N-methyl-p-toluenesulfonylamide (640-61-9) → N,4-dimethyl-N-(oxiran-2-ylmethyl)benzenesulfonamide (890662-14-3)

Guidance literature:

for 48h; Product distribution / selectivity; Heating / reflux;

upstream raw materials:

epichlorohydrin

N-methyl-p-toluenesulfonylamide

N-allyl-N-methyl-4-toluene sulphonamide

1,2-Epoxy-3-bromopropane

Downstream raw materials:

N-(3-hydroxyprop-1-enyl)-N,4-dimethylbenzenesulfonamide

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