(4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

Base Information

Chemical Name:(4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)
CAS No.:1236350-51-8
Molecular Formula:C₄₄H₃₅ClN₄Pt
Molecular Weight:850.322
Hs Code.:

Synonyms:(4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

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Chemical Property of (4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

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Technology Process of (4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

There total 1 articles about (4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.4%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 1236350-50-7
4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine

: 1236350-51-8
(4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

Guidance literature:: In acetic acid; org. ligand (0.5 mmol), K2PtCl4 (0.5 mmol) and glacial acetic acid (30 ml) refluxed (24 h, N2, in the dark); cooled to room temp.; filtered; recrystd. from MeOH/CH2Cl2; elem. anal.;
DOI:10.1016/j.electacta.2011.11.083

Reference yield: 87.0%

: 1236350-51-8
(4-[p-[N-(4-(9-carbazole))butyl-N-phenyl]aniline]-6-phenyl-2,2'-bipyridine)chloridoplatinum(II)

: 536-74-3
phenylacetylene

: 1356958-89-8
[(4-(p-[N-(4-(9-carbazole)butyl)-N-phenyl]amino)-6-phenyl-2,2'-bipyridine-H)Pt(C₂(C₆H₅))]

Guidance literature:: With CuI; Et₃N; In dichloromethane; mixt. of Pt complex (0.30 mmol), C6H5C2H (1 mmol), Et3N (5 ml) and CuI (5 mg) in degassed CH2Cl2 (50 ml) stirred (12 h, under N2, in the dark); evapd. to dryness (vac.); flash chromy. (neutral Al2O3, CH2Cl2); recrystd. from CH2Cl2/MeOH;
DOI:10.1016/j.electacta.2011.11.083