N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

Base Information

Chemical Name:N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide
CAS No.:80780-59-2
Molecular Formula:C₃₃H₄₀N₄O₁₀
Molecular Weight:652.701
Hs Code.:

Synonyms:N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

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Technology Process of N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

There total 3 articles about N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 3223-20-9
5-nitrosalicyloyl chloride

: 80764-58-5
Butyl-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-amine

: 80780-59-2
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/ja00371a028

Reference yield:

: 53408-96-1
4'-nitrobenzo-18-crown-6

: 80780-59-2
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd-C

2: 1.) NaNO₂, aq. HCl / 2.) room temperature, 1 d

3: 17 percent / NaHCO₃ / tetrahydrofuran / Ambient temperature

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/ja00371a028

Reference yield:

: 80764-63-2
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

: 80780-59-2
N-Butyl-N-[4-(6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-benzocyclooctadecen-2-ylazo)-phenyl]-2-hydroxy-5-nitro-benzamide

Guidance literature:: In 1,2-dichloro-benzene; tert-butyl alcohol; at 30 ℃; Rate constant; thermal isomerization, influence of alkali metal cations; extraction of alkali and alkali earth metal cations; rate of ion transport across a liquid membrane;
DOI:10.1021/ja00371a028