Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

Base Information

Chemical Name:Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate
CAS No.:150920-81-3
Molecular Formula:C₂₄H₂₆BrNO₁₅
Molecular Weight:648.372
Hs Code.:

Synonyms:Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

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Chemical Property of Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

Chemical Property:

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Technology Process of Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

There total 6 articles about Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 150920-80-2
methyl [4,5,7,8-tetra-O-acetyl-2,3-di-O-(4-nitrobenzoyl)-D-glycero-α-D-talo-oct-2-ulopyranos]onate

: 150920-81-3
Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

Guidance literature:: With titanium(IV) bromide; In dichloromethane; for 48h; Heating;
DOI:10.1016/0008-6215(93)80005-Y

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 150920-81-3
Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

Guidance literature:: Multi-step reaction with 2 steps

2: 100 percent / TiBr₄ / CH₂Cl₂ / 48 h / Heating

With titanium(IV) bromide; In dichloromethane;
DOI:10.1016/0008-6215(93)80005-Y

Reference yield:

: 85382-90-7
methyl-4,5,7,8-tetra-O-acetyl-2,6-anhydro-2,3-dideoxy-D-manno-oct-2-enosonat

: 150920-81-3
Methyl <4,5,7,8-tetra-O-acetyl-3-O-(4-nitrobenzoyl)-α-D-glycero-D-talo-2-octulopyranosyl bromide>onate

Guidance literature:: Multi-step reaction with 2 steps

2: 100 percent / TiBr₄ / CH₂Cl₂ / 48 h / Heating

With titanium(IV) bromide; In dichloromethane;
DOI:10.1016/0008-6215(93)80005-Y