8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

Base Information

Chemical Name:8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline
CAS No.:170948-55-7
Molecular Formula:C₂₃H₂₂ClN₅O
Molecular Weight:419.914
Hs Code.:

Synonyms:8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

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Chemical Property of 8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

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Technology Process of 8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

There total 6 articles about 8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 160461-82-5
8,10-dichloropyrido<3,2-f>quinoxaline

: 69019-09-6
4-hydroxy-3-piperidinomethylaniline

: 170948-55-7
8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

Guidance literature:: In diethylene glycol dimethyl ether; at 130 ℃; for 3h;

Reference yield:

: 70039-10-0
10-oxo-7,10-dihydro-pyrido[3,2-f]quinoxaline-9-carboxylic acid ethyl ester

: 170948-55-7
8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

Guidance literature:: Multi-step reaction with 6 steps

1: 5percent aq. NaOH / 1 h / Heating

2: quinoline / 2 h / Heating

3: 61 percent / POCl₃ / 4 h / Heating

4: 81 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature

5: 63 percent / POCl₃ / 1 h / Heating

6: 19 percent / bis-(2-methoxy-ethyl) ether / 3 h / 130 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In quinoline; dichloromethane; diethylene glycol dimethyl ether;

Reference yield:

: 70039-11-1
10-oxo-7,10-dihydro-pyrido[3,2-f]quinoxaline-9-carboxylic acid

: 170948-55-7
8-chloro-10-(4-hydroxy-3-piperidinomethyl)anilinopyrido<3,2-f>quinoxaline

Guidance literature:: Multi-step reaction with 5 steps

1: quinoline / 2 h / Heating

2: 61 percent / POCl₃ / 4 h / Heating

3: 81 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature

4: 63 percent / POCl₃ / 1 h / Heating

5: 19 percent / bis-(2-methoxy-ethyl) ether / 3 h / 130 °C

With 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In quinoline; dichloromethane; diethylene glycol dimethyl ether;