Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

Base Information

• Chemical Name: Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid
• CAS No.: 113879-98-4
• Molecular Formula: C₄₆H₄₇Br₃O₁₃
• Molecular Weight: 1047.58

Synonyms:Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

Chemical Property of Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

Chemical Property:

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Technology Process of Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

There total 10 articles about Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-3-O-formyl-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid (108365-30-6) → Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid (113879-98-4)

Guidance literature:

With hydrogenchloride; methanol;

Reference yield:

4-O-Benzoyl-2-brom-2,6-didesoxy-3-O-formyl-α-D-clucopyranosylbromid (85726-77-8) → Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid (113879-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1: molecular sieves 4A, silver trifluoromethanesulfonate / nitromethane; toluene / 48 h / -78 °C

2: 80 percent / HCl / CH₂Cl₂; methanol / 6 h / Ambient temperature

With hydrogenchloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In methanol; nitromethane; dichloromethane; toluene;

DOI:10.1016/0008-6215(87)80139-8

Reference yield:

Benzyl-4-O-benzoyl-3-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-d-glucopyranosyl)-2-brom-2,6-didesoxy-β-D-glucopyranosid (108319-57-9) → Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid (113879-98-4)

Guidance literature:

Multi-step reaction with 2 steps

1: molecular sieves 4A, silver trifluoromethanesulfonate / nitromethane; toluene / 48 h / -78 °C

2: 80 percent / HCl / CH₂Cl₂; methanol / 6 h / Ambient temperature

With hydrogenchloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In methanol; nitromethane; dichloromethane; toluene;

DOI:10.1016/0008-6215(87)80139-8

upstream raw materials:

Benzyl-O-(4-O-benzoyl-2-brom-2,6-didesoxy-3-O-formyl-β-D-glucopyranosyl)-(1->3)-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosyl)-(1->3)-4-O-benzoyl-2-brom-2,6-didesoxy-β-D-glucopyranosid

4-O-Benzoyl-2-brom-2,6-didesoxy-3-O-formyl-α-D-clucopyranosylbromid

Benzyl-4-O-benzoyl-3-O-(4-O-benzoyl-2-brom-2,6-didesoxy-β-d-glucopyranosyl)-2-brom-2,6-didesoxy-β-D-glucopyranosid

C₃₄H₃₄Br₂O₁₀

Downstream raw materials:

Benzyl-O-(4-O-benzoyl-2,6-didesoxy-β-D-erythro-hexopyranosid-3-ulose)-(1->3)-O-(4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

benzyl 4-O-benzoyl-3-O-[4-O-benzoyl-3-O-(3-C-methylen-2,3,6-trideoxy-β-D-erythro-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl]-2,6-dideoxy-β-D-arabino-hexopyranoside

benzyl 4-O-benzoyl-3-O-[4-O-benzoyl-3-O-(3,3'-anhydro-2,6-dideoxy-3-C-hydroxymethyl-β-D-ribo-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl]-2,6-dideoxy-β-D-arabino-hexopyranoside

benzyl 3-O-[3-O-(2,6-dideoxy-3-C-methyl-β-D-ribo-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranosyl]-2,6-dideoxy-β-D-arabino-hexopyranoside

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