(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

Base Information

Chemical Name:(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane
CAS No.:1346167-11-0
Molecular Formula:C₃₁H₃₃N₃O₆
Molecular Weight:543.62
Hs Code.:

Synonyms:(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

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Chemical Property of (1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

Chemical Property:

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Technology Process of (1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

There total 1 articles about (1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1208102-25-3
(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

: 108-24-7
acetic anhydride

: 1346167-11-0
(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

Guidance literature:: With acetic acid; zinc(II) chloride; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c1ob06038d

Reference yield: 85.0%

: 1346167-11-0
(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

: 1346167-12-1
(1R,2R,3R,4R,5R)-5-azido-2,3-di-O-benzyl-4-C-hydroxymethylcycloheptanol

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob06038d

Reference yield:

: 1346167-11-0
(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

: 1346167-13-2
C₂₂H₂₃N₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 20 °C / Inert atmosphere

2: Jones reagent / water; acetone / 3 h / 0 °C / Inert atmosphere

With Jones reagent; sodium methylate; In methanol; water; acetone;
DOI:10.1039/c1ob06038d