(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

Base Information

Chemical Name:(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane
CAS No.:1208102-25-3
Molecular Formula:C₃₆H₃₇N₃O₅
Molecular Weight:591.707
Hs Code.:

Synonyms:(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

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Chemical Property of (1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

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Technology Process of (1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

There total 1 articles about (1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1208102-24-2
(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

: 1208102-25-3
(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

Guidance literature:: (1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With diphenyl phosphoryl azide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b918576c

Reference yield: 74.0%

: 1208102-25-3
(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

: 108-24-7
acetic anhydride

: 1346167-11-0
(1R,2R,3R,4R,5R)-4-(acetoxymethyl)-5-azido-1-O-benzoyl-2,3-di-O-benzylcycloheptane

Guidance literature:: With acetic acid; zinc(II) chloride; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c1ob06038d

Reference yield:

: 1208102-25-3
(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

: 1346167-13-2
C₂₂H₂₃N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; zinc(II) chloride / 3 h / 20 °C / Inert atmosphere

2: sodium methylate / methanol / 20 °C / Inert atmosphere

3: Jones reagent / water; acetone / 3 h / 0 °C / Inert atmosphere

With Jones reagent; sodium methylate; acetic acid; zinc(II) chloride; In methanol; water; acetone;
DOI:10.1039/c1ob06038d